UC Davis NMR Equipment

800 MHz Bruker Avance III Spectrometer with TCI Cryoprobe at the UC Davis NMR Facility

800 MHz Bruker Avance III Spectrometer with TCI Cryoprobe

The UC Davis Nuclear Magnetic Resonance (NMR) Facility is equipped with state-of-the-art magnetic resonance equipment suitable for liquids, solids and imaging experiments.  Below is a short summary of our available instrumentation.  You can see more information about each spectrometer by clicking on the tabs to the left.

MedSci-1D

The MedSci-1D Facility houses 600 and 800 MHz Bruker Avance III spectrometers, both usually equipped with cryoprobes for increased sensitivity over conventional NMR probes.  These cryoprobes are ideally suited for NMR structure determination of proteins, nucleic acids and other biomolecules.

The 500 MHz Bruker Avance DRX spectrometer is usually equipped with a 5 mm 1H/BB probe with an X-channel tunable from 15N to 31P. This spectrometer is also capable of both low-temperature and high-temperature experiments, and has an automatic sample changer for high-throughput work.

At MedSci we have 2 spectrometers capable of MRI / Imaging. The 400 MHz Bruker DRX spectrometer is a vertical-bore instrument with both spectroscopy and microimaging capabilities, and has both Topspin and Paravision 4 software for spectrometer control. The 7T (300 MHz) MRI instrument is a horizontal-bore spectrometer ideal for small-animal imaging.

Chemistry

Chemistry room 93 houses 2 NMR Varian spectrometers using VnmrJ software and 1 Bruker NMR spectrometer.  The instrument of choice for most organic/inorganic chemists interested in routine 1D and 2D NMR experiments is the 400 MHz Bruker spectrometer in room 93. This spectrometer is equipped with a 5 mm 1H/X broadband probe with autotuning/automatching capabilities.  

Chemistry room 3470 (Chem Annex) is home to a single Mercury Plus spectrometer (Varian) primarily used for teaching purposes.  

Kemper Hall

Kemper Hall room 51 is the home to the 500 MHz BRUKER AVANCE I NMR spectrometer equipped with an 11.74T wide bore Bruker magnet specifically designated for solid-state-NMR experiments. Depending on the features of the researchers’ projects, various probes are available with difference sample sizes ad spinning speeds. The 2.5, and 7 mm probes are H/BB CPMAS probes with the broadband tunes to 15N-31P. A 4mm triple-resonance (H/BB/BB) CPMAS probe is cable of running X-Y correlation MAS NMR experiments, for example, H/N/C, H/C/P, H/Si/Al. The 4 mm and 7 mm log-gamma CPMAS probes cover the frequency range of 12-50MHz (41K – 51N). The wideline probe is capable of running static NMR experiment at VT range of -150C to 400C, and covers the frequency range from 109Ag to 31P.

Scheduling

Trained users can reserve NMR experiment time by visiting our Online Scheduler

Supplemental content

NMR Facility Information

NMR Facility Staff

Prof. Gary Smith - Director, NMR Facility

530-752-6168

gmsmith@ucdavis.edu

Dr. Jeff WaltonMRI / Imaging and Misc. NMR

530-752-7794

jhwalton@ucdavis.edu

Dr. Ping Yu - Liquids and Solids NMR

530-752-4396

pyu@ucdavis.edu